
A test method for N-vinylpyrrolidone includes the following steps: 1) sample solution and reference solution to prepare sample solution: weigh the sample in a glass bottle, grind it into powder, add 5 ~ 15 times the weight of the extractant, ultrasonic extraction for 20 ~ 40min, centrifuge separation, take the supernatant and filter it, obtain the filtrate, and reserve; Reference solution: Take N-vinylpyrrolidone reference product, one weight of the same extraction agent as the sample solution, shake well, set aside; 2) Liquid chromatograph conditional column: SFC capillary Chemicalbook column; Stationary phase: octadecylsilane bonded silica gel as the filling column; Column temperature: 36-38ºC, sample volume: 20-30μL; Mobile phase: C2H3N-N2O-CH4O with volume ratio of 5:3:50 is used as mobile phase; Detection wavelength: 200 ~ 215nm; Constant pressure: 65.7×106Pa; The flow rate was 1 ~ 1.5ml/min. Detection point: FID, 250ºC; Replenishing gas: nitrogen; 3) Determination Absorb the reference solution and the sample solution respectively, and inject the liquid chromatograph for determination.








